TA Instruments

AR1772-0002f

28/03/2013 12:45:47

Sample name	DI 40 mm AL blank plate 10 mm gap
Sample notes	 
Experiment notes	DI Deionised water, 40 mm diameter. 70 mm total depth of water, 10 mm gap, with PE beads
Operator	mr1
Sample density	1.000 g/cm^3
Results file name	AR1772
Run number	2 
Results directory	D:\ARG2 rheometer\Test files\Southampton University P Stoodley May2012
Experiment was run on	28/03/2013 12:45:47

Procedure name	Flow procedure
Procedure notes	

Step name	Conditioning Step 1
Step notes	
Perform step	Yes
Initial temperature	20.0 C
Wait for correct temperature	Yes
Do set temperature	Yes
Wait for normal force	No
Perform pre-shear	No
Perform equilibration	Yes
Equilibration duration	0:00:30 hh:mm:ss
Wait for zero velocity	No
Control normal force	Uses current instrument settings
Purge gas only	No

Step name	Continuous ramp step 1
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 3.000 rad/s
End controlled variable	velocity 300.0 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	20.0 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Peak hold step
Step notes	
Perform step	Yes
Ramp type	Peak hold
Controlled variable	velocity 300.0 rad/s
Duration	0:01:00 hh:mm:ss
Delay time	0:00:01 hh:mm:ss
Temperature	20.0 C
Wait for temperature	No
Motor mode	auto 

Step name	Continuous ramp step 2
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 300.0 rad/s
End controlled variable	velocity 3.000 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	20.0 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Post-Experiment Step
Step notes	
Perform step	Yes
Do set temperature	Yes
Temperature	20.0 C
Set temperature system idle	No

Geometry name	40 mm ETC AL plate with studs
Geometry notes	Standard ETC AL parallel plate with studs
Geometry material	Aluminum
Parallel plate diameter	40.00 mm
gap	10000 micro m
Gap offset	0 micro m
Geometry inertia	2.056 micro N.m.s^2
Geometry compliance	3.130E-3 rad/N.m
Gap temperature compensation	0 micro m/C
Gap temperature compensation enabled	No
Shear rate factor	2.000 
Shear stress factor	79580 1/m^3
Measurement system factor	39790 1/m^3
Fluid density factor	8.378E-10 m^5
Normal force factor	1592 1/m^2
Backoff distance	26500 micro m
Approximate sample volume	12.57 ml

Sample compression	linear 
Compression distance	1000.0 micro m
Compression velocity	50.0 micro m/s
Fine velocity	500.0 micro m/s
Coarse velocity	6000.0 micro m/s
Other velocity	6000.0 micro m/s
Current temperature system	Peltier plate
Temperature control	Enabled 
Purge gas only	No
Temperature calibration	Peltier plate - 0.6 micro m/C
	Water bath - 0 micro m/C
	Torsion oven - plate - 0 micro m/C
	Torsion oven - solid sample - 0 micro m/C
	Peltier concentric cylinders - 0 micro m/C
	None - 0 micro m/C
	Stress relaxation - 0 micro m/C
	Current temperature system - 0 micro m/C
Cooling water temperature	15.0 C
Cooling water range	6.0 C
Bearing friction correction	Yes
Bearing friction	0.261 micro N.m/(rad/s)
Bearing offset	0 micro N.m
Temperature system span and offset	Peltier plate - span 1.0000 , offset 0 C
	Water bath - span 1.0000 , offset 0 C
	Torsion oven - plate - span 1.0000 , offset 0 C
	Torsion oven - solid sample - span 1.0000 , offset 0 C
	Peltier concentric cylinders - span 1.0000 , offset 0 C
	None - span 1.0000 , offset 0 C
	Stress relaxation - span 1.0000 , offset 0 C
	Current temperature system - span 1.0000 , offset 0 C
Bearing mapping type	precision 
Number of mapping iterations	1
Instrument type (MType)	AR-G2
Firmware version	  8.29  27/10/09
Configuration version (CnfVer)	301
Parameter version (PrmVer)	301
PCB Number	*NOT_SET*
IP address	192.168.1.2
Software version	V5.8.0
Windows version	Windows XP 5.1 (Service Pack 2)
Instrument inertia	21.01 micro N.m.s^2
Auto increment run number	Yes
Prompt for file name at start of run	Yes
Auto save results file	Yes
Results file storage	Consecutive steps of same type to 1 file 
Temperature tolerance	0.2 C
Temperature duration	0:00:10 hh:mm:ss
Wait for temperature even if OK	Yes
Gap tolerance	4 micro m
Gap duration	0:00:02 hh:mm:ss
Override wait for gap	No
Velocity tolerance	0.1000 rad/s
Zero speed after pre-shear	Leave as is 
Zero normal force before run	No
Zero timer before run	Before pre-shear 
Non-equilibrium minimum velocity	1.000E-4 rad/s
Zero strain at the start of each flow step	Yes
Inertia correction	Yes
Collect negative shear rate data if stress is positive	Yes
Collect all points	No
Display flow point graph during run	Yes
Store flow point graph with results	Yes
Store images to the results for flow steps	Yes
Creep zero displacement	Yes
Store images to the results for creep steps	Yes
Standard creep image store frequency	10 s
Repeated creep image store frequency in repeats	10 
Display oscillation waveform graph during run	Yes
Store oscillation waveform graph with results	Yes
Display strain control tries during run	Yes
Store strain control tries with results	Yes
Store images to the results for oscillation steps	Yes
Stress relaxation zero displacement	Yes
Store images to the results for stress relaxation steps	Yes
Flow torque limit	10.00 micro N.m
Flow velocity limit	1.000E-3 rad/s
Oscillation torque limit	5.00 micro N.m
Oscillation displacement limit	1.00E-5 rad
Oscillation raw phase limit	170.0 degrees
Oscillation minimum normal force limit	0.1000 N
Oscillation maximum normal force limit	50.00 N
Flow velocity tolerance	1.00 %
Oscillation torque tolerance	1.00 %
Oscillation displacement tolerance	1.00 %
Oscillation velocity tolerance	1.00 %
Temperature tolerance	1.0 C

Continuous ramp step 1

time	velocity	torque	gap	temperature	normal force	time global	shear stress	shear rate	viscosity	normal stress	displacement	normal stress coefficient	strain	% strain	1/temperature	time	time global
s	rad/s	micro N.m	micro m	C	N	s	Pa	1/s	Pa.s	Pa	rad	Pa.s^2			1/K	min	min

1.0040	4.217	-10.707	10000	20.0	5.843	31.004	-0.8520	8.434	-0.1010	9299	1.7834	130.7	3.5667	356.67	3.411E-3	0.0	0.5
2.0080	10.02	11.803	10000	20.0	5.843	32.008	0.9393	20.03	0.04688	9300	13.7187	23.17	27.437	2743.7	3.411E-3	0.0	0.5
3.0160	15.55	22.136	10000	20.0	5.842	33.016	1.762	31.11	0.05662	9298	27.1309	9.608	54.262	5426.2	3.411E-3	0.1	0.6
4.0200	18.48	29.272	10000	20.0	5.845	34.020	2.329	36.97	0.06301	9302	41.0650	6.806	82.130	8213.0	3.411E-3	0.1	0.6
5.0160	24.72	45.072	10000	20.0	5.845	35.016	3.587	49.43	0.07256	9303	67.9279	3.807	135.86	13586	3.411E-3	0.1	0.6
6.0240	31.61	66.603	10000	20.0	5.844	36.024	5.300	63.23	0.08382	9301	107.1030	2.326	214.21	21421	3.411E-3	0.1	0.6
7.0160	34.05	74.547	10000	20.0	5.840	37.016	5.932	68.10	0.08711	9294	126.4590	2.004	252.92	25292	3.411E-3	0.1	0.6
8.0160	39.32	92.047	10000	20.0	5.838	38.016	7.325	78.65	0.09313	9292	165.4090	1.502	330.82	33082	3.411E-3	0.1	0.6
9.0160	46.05	117.57	10000	20.0	5.833	39.016	9.356	92.10	0.1016	9283	223.3590	1.094	446.72	44672	3.411E-3	0.2	0.7
10.016	50.97	138.07	10000	20.0	5.827	40.016	10.99	101.9	0.1078	9274	274.9310	0.8923	549.86	54986	3.411E-3	0.2	0.7
11.016	55.74	160.04	10000	20.0	5.822	41.016	12.74	111.5	0.1142	9266	326.2210	0.7456	652.44	65244	3.411E-3	0.2	0.7
12.008	60.11	179.11	10000	20.0	5.821	42.008	14.25	120.2	0.1186	9264	377.4320	0.6409	754.86	75486	3.411E-3	0.2	0.7
13.020	64.43	198.74	10000	20.0	5.816	43.020	15.82	128.9	0.1227	9257	435.1660	0.5575	870.33	87033	3.411E-3	0.2	0.7
14.020	69.16	223.40	10000	20.0	5.815	44.020	17.78	138.3	0.1285	9254	498.8330	0.4837	997.67	99767	3.411E-3	0.2	0.7
15.000	75.69	258.77	10000	20.0	5.806	45.000	20.59	151.4	0.1360	9241	594.7790	0.4032	1189.6	1.1896E5	3.411E-3	0.3	0.8
16.016	79.94	280.49	10000	20.0	5.808	46.016	22.32	159.9	0.1396	9243	664.4120	0.3616	1328.8	1.3288E5	3.411E-3	0.3	0.8
17.016	84.54	306.98	10000	20.0	5.797	47.016	24.43	169.1	0.1445	9227	740.9670	0.3228	1481.9	1.4819E5	3.411E-3	0.3	0.8
18.020	90.99	344.06	10000	20.0	5.791	48.020	27.38	182.0	0.1505	9217	855.3990	0.2783	1710.8	1.7108E5	3.411E-3	0.3	0.8
19.016	95.05	366.59	10000	20.0	5.785	49.016	29.17	190.1	0.1535	9207	931.3170	0.2548	1862.6	1.8626E5	3.411E-3	0.3	0.8
20.016	99.41	395.57	10000	20.0	5.784	50.016	31.48	198.8	0.1583	9205	1020.3000	0.2329	2040.6	2.0406E5	3.411E-3	0.3	0.8
21.016	105.8	438.40	10000	20.0	5.772	51.016	34.89	211.7	0.1648	9186	1153.5900	0.2050	2307.2	2.3072E5	3.411E-3	0.4	0.9
22.016	109.9	468.50	10000	20.0	5.762	52.016	37.28	219.8	0.1696	9170	1242.2500	0.1898	2484.5	2.4845E5	3.411E-3	0.4	0.9
23.020	114.2	490.02	10000	20.0	5.761	53.020	38.99	228.5	0.1707	9169	1344.2300	0.1756	2688.5	2.6885E5	3.411E-3	0.4	0.9
24.016	120.7	532.67	10000	20.0	5.753	54.016	42.39	241.3	0.1757	9156	1495.8300	0.1572	2991.7	2.9917E5	3.411E-3	0.4	0.9
25.016	124.7	557.72	10000	20.0	5.746	55.016	44.38	249.5	0.1779	9146	1597.0699	0.1469	3194.1	3.1941E5	3.411E-3	0.4	0.9
26.016	129.1	595.47	10000	20.0	5.738	56.016	47.39	258.1	0.1836	9132	1711.1700	0.1371	3422.3	3.4223E5	3.411E-3	0.4	0.9
27.016	135.5	640.75	10000	20.0	5.729	57.016	50.99	270.9	0.1882	9119	1882.0800	0.1242	3764.2	3.7642E5	3.411E-3	0.5	1.0
28.016	139.6	668.30	10000	20.0	5.724	58.016	53.18	279.1	0.1905	9110	1995.9900	0.1169	3992.0	3.9920E5	3.411E-3	0.5	1.0
29.016	143.6	694.42	10000	20.0	5.718	59.016	55.26	287.3	0.1924	9100	2118.3501	0.1103	4236.7	4.2367E5	3.411E-3	0.5	1.0
30.016	150.0	751.71	10000	20.0	5.708	60.016	59.82	300.1	0.1993	9085	2305.8899	0.1009	4611.8	4.6118E5	3.411E-3	0.5	1.0
31.000	154.2	777.50	10000	20.0	5.697	61.000	61.87	308.3	0.2007	9068	2433.5500	0.09539	4867.1	4.8671E5	3.411E-3	0.5	1.0
32.012	160.4	814.07	10000	20.0	5.689	62.012	64.78	320.8	0.2019	9054	2635.5701	0.08795	5271.1	5.2711E5	3.411E-3	0.5	1.0
33.016	164.7	860.19	10000	20.0	5.683	63.016	68.45	329.3	0.2078	9044	2774.5601	0.08338	5549.1	5.5491E5	3.411E-3	0.6	1.1
34.016	168.8	903.60	10000	20.0	5.672	64.016	71.91	337.6	0.2130	9028	2912.6699	0.07922	5825.3	5.8253E5	3.411E-3	0.6	1.1
35.020	174.9	949.38	10000	20.0	5.663	65.020	75.55	349.8	0.2160	9013	3127.5701	0.07368	6255.1	6.2551E5	3.411E-3	0.6	1.1
36.000	179.1	993.87	10000	20.0	5.662	66.000	79.09	358.2	0.2208	9011	3279.1599	0.07022	6558.3	6.5583E5	3.411E-3	0.6	1.1
37.016	183.2	1037.4	10000	20.0	5.650	67.016	82.55	366.5	0.2252	8992	3430.8601	0.06695	6861.7	6.8617E5	3.411E-3	0.6	1.1
38.016	189.3	1078.8	10000	20.0	5.635	68.016	85.85	378.6	0.2268	8969	3658.0801	0.06257	7316.2	7.3162E5	3.412E-3	0.6	1.1
39.020	193.5	1107.3	10000	20.0	5.630	69.020	88.12	386.9	0.2277	8960	3822.6899	0.05985	7645.4	7.6454E5	3.411E-3	0.7	1.2
40.016	199.7	1175.4	10000	20.0	5.610	70.016	93.54	399.3	0.2342	8928	4068.5500	0.05599	8137.1	8.1371E5	3.411E-3	0.7	1.2
41.000	203.7	1209.9	10000	20.0	5.598	71.000	96.28	407.4	0.2363	8909	4232.6299	0.05368	8465.3	8.4653E5	3.411E-3	0.7	1.2
42.016	210.0	1250.9	10000	20.0	5.595	72.016	99.55	419.9	0.2371	8905	4499.5801	0.05050	8999.2	8.9992E5	3.411E-3	0.7	1.2
43.008	214.1	1302.6	10000	20.0	5.580	73.008	103.7	428.2	0.2421	8880	4674.5698	0.04844	9349.1	9.3491E5	3.411E-3	0.7	1.2
44.024	218.1	1367.6	10000	20.0	5.572	74.024	108.8	436.2	0.2495	8868	4851.2700	0.04660	9702.5	9.7025E5	3.411E-3	0.7	1.2
45.000	224.3	1399.2	10000	20.0	5.567	75.000	111.3	448.6	0.2482	8860	5129.0200	0.04403	10258	1.0258E6	3.411E-3	0.8	1.3
46.016	228.4	1448.0	10000	20.0	5.553	76.016	115.2	456.8	0.2522	8838	5319.0098	0.04235	10638	1.0638E6	3.411E-3	0.8	1.3
47.020	234.5	1515.1	10000	20.0	5.555	77.020	120.6	468.9	0.2571	8842	5609.2900	0.04021	11219	1.1219E6	3.411E-3	0.8	1.3
48.016	238.6	1541.9	10000	20.0	5.534	78.016	122.7	477.3	0.2571	8807	5803.8198	0.03867	11608	1.1608E6	3.411E-3	0.8	1.3
49.016	242.8	1601.2	10000	20.0	5.515	79.016	127.4	485.5	0.2624	8778	6005.6001	0.03724	12011	1.2011E6	3.411E-3	0.8	1.3
50.000	248.9	1649.0	10000	20.0	5.508	80.000	131.2	497.8	0.2636	8766	6311.4600	0.03538	12623	1.2623E6	3.411E-3	0.8	1.3
51.016	252.9	1681.9	10000	20.0	5.484	81.016	133.8	505.9	0.2646	8728	6518.5698	0.03411	13037	1.3037E6	3.411E-3	0.9	1.4
52.008	259.2	1747.3	10000	20.0	5.472	82.008	139.0	518.4	0.2682	8710	6841.8398	0.03242	13684	1.3684E6	3.411E-3	0.9	1.4
53.016	263.2	1783.4	10000	20.0	5.470	83.016	141.9	526.4	0.2696	8706	7052.4800	0.03142	14105	1.4105E6	3.411E-3	0.9	1.4
54.020	269.2	1884.0	10000	20.0	5.448	84.020	149.9	538.5	0.2784	8671	7380.4800	0.02990	14761	1.4761E6	3.411E-3	0.9	1.4
55.000	273.4	1895.6	10000	20.0	5.451	85.000	150.9	546.7	0.2759	8676	7607.8301	0.02902	15216	1.5216E6	3.411E-3	0.9	1.4
56.016	277.4	1968.0	10000	20.0	5.442	86.016	156.6	554.9	0.2822	8661	7834.4800	0.02813	15669	1.5669E6	3.411E-3	0.9	1.4
57.016	283.5	2033.4	10000	20.0	5.431	87.016	161.8	567.0	0.2854	8644	8175.9302	0.02689	16352	1.6352E6	3.411E-3	1.0	1.5
57.996	287.6	2061.8	10000	20.0	5.425	87.996	164.1	575.1	0.2853	8634	8414.5596	0.02610	16829	1.6829E6	3.411E-3	1.0	1.5
59.016	293.7	2135.1	10000	20.0	5.398	89.016	169.9	587.4	0.2893	8591	8776.0098	0.02490	17552	1.7552E6	3.411E-3	1.0	1.5
60.016	297.7	2189.4	10000	20.0	5.381	90.016	174.2	595.4	0.2926	8565	9013.3203	0.02416	18027	1.8027E6	3.411E-3	1.0	1.5

Peak hold step

time	velocity	torque	gap	temperature	normal force	time global	shear stress	shear rate	viscosity	normal stress	displacement	normal stress coefficient	strain	% strain	1/temperature	time	time global
s	rad/s	micro N.m	micro m	C	N	s	Pa	1/s	Pa.s	Pa	rad	Pa.s^2			1/K	min	min

0.99600	300.0	2210.7	10000	20.0	5.366	91.996	175.9	600.0	0.2932	8540	294.5430	0.02372	589.09	58909	3.411E-3	0.0	1.5
1.9960	300.0	2203.0	10000	20.0	5.371	92.996	175.3	600.0	0.2922	8547	542.6700	0.02375	1085.3	1.0853E5	3.411E-3	0.0	1.5
3.0000	300.0	2214.2	10000	20.0	5.371	94.000	176.2	600.0	0.2937	8548	919.5130	0.02375	1839.0	1.8390E5	3.411E-3	0.1	1.6
4.0000	300.0	2200.7	10000	20.0	5.386	95.000	175.1	600.0	0.2919	8572	1182.2500	0.02381	2364.5	2.3645E5	3.412E-3	0.1	1.6
4.9960	300.0	2191.2	10000	20.0	5.374	95.996	174.4	600.0	0.2906	8553	1422.0900	0.02376	2844.2	2.8442E5	3.411E-3	0.1	1.6
5.9960	300.0	2204.6	10000	20.0	5.384	96.996	175.4	600.1	0.2924	8568	1799.1100	0.02379	3598.2	3.5982E5	3.411E-3	0.1	1.6
6.9960	300.0	2195.7	10000	20.0	5.365	97.996	174.7	600.1	0.2912	8539	2050.3401	0.02371	4100.7	4.1007E5	3.411E-3	0.1	1.6
7.9960	300.0	2204.8	10000	20.0	5.358	98.996	175.5	600.0	0.2924	8527	2301.8799	0.02369	4603.8	4.6038E5	3.411E-3	0.1	1.6
8.9960	300.0	2205.9	10000	20.0	5.364	99.996	175.5	600.0	0.2926	8536	2680.5200	0.02371	5361.0	5.3610E5	3.411E-3	0.1	1.7
9.9960	300.0	2223.3	10000	20.0	5.387	100.996	176.9	600.0	0.2949	8573	2930.2200	0.02382	5860.4	5.8604E5	3.411E-3	0.2	1.7
10.996	300.0	2196.4	10000	20.0	5.375	101.996	174.8	600.0	0.2913	8555	3307.8799	0.02376	6615.8	6.6158E5	3.411E-3	0.2	1.7
11.996	300.0	2207.1	10000	20.0	5.368	102.996	175.6	600.0	0.2927	8543	3558.3899	0.02373	7116.8	7.1168E5	3.411E-3	0.2	1.7
12.996	299.9	2227.0	10000	20.0	5.369	103.996	177.2	599.9	0.2954	8546	3809.7400	0.02375	7619.5	7.6195E5	3.411E-3	0.2	1.7
14.000	300.0	2213.7	10000	20.0	5.357	105.000	176.2	600.0	0.2936	8526	4186.7598	0.02368	8373.5	8.3735E5	3.411E-3	0.2	1.8
14.996	300.0	2219.5	10000	20.0	5.376	105.996	176.6	600.0	0.2944	8557	4438.2100	0.02377	8876.4	8.8764E5	3.411E-3	0.2	1.8
16.000	300.0	2222.4	10000	20.0	5.356	107.000	176.9	599.9	0.2948	8524	4815.1299	0.02368	9630.3	9.6303E5	3.411E-3	0.3	1.8
16.996	300.0	2180.7	10000	20.0	5.377	107.996	173.5	600.1	0.2892	8558	5066.4702	0.02377	10133	1.0133E6	3.411E-3	0.3	1.8
17.996	300.0	2203.7	10000	20.0	5.385	108.996	175.4	600.1	0.2922	8570	5317.6499	0.02380	10635	1.0635E6	3.411E-3	0.3	1.8
18.996	300.0	2209.4	10000	20.0	5.375	109.996	175.8	600.0	0.2930	8555	5696.4702	0.02376	11393	1.1393E6	3.411E-3	0.3	1.8
19.996	300.0	2207.3	10000	20.0	5.381	110.996	175.7	600.0	0.2928	8565	5945.9600	0.02379	11892	1.1892E6	3.411E-3	0.3	1.8
20.996	300.0	2243.6	10000	20.0	5.374	111.996	178.5	600.1	0.2975	8553	6326.3999	0.02375	12653	1.2653E6	3.411E-3	0.3	1.9
21.996	300.0	2201.4	10000	20.0	5.380	112.996	175.2	600.0	0.2920	8563	6578.3901	0.02379	13157	1.3157E6	3.411E-3	0.4	1.9
22.996	300.0	2193.9	10000	20.0	5.380	113.996	174.6	600.0	0.2910	8563	6836.6201	0.02378	13673	1.3673E6	3.411E-3	0.4	1.9
23.996	300.0	2192.5	10000	20.0	5.376	114.996	174.5	600.0	0.2908	8556	7203.2002	0.02376	14406	1.4406E6	3.411E-3	0.4	1.9
24.996	300.0	2187.0	10000	20.0	5.377	115.996	174.0	600.1	0.2900	8558	7457.3999	0.02376	14915	1.4915E6	3.411E-3	0.4	1.9
25.996	300.0	2204.3	10000	20.0	5.388	116.996	175.4	600.0	0.2923	8575	7705.3398	0.02382	15411	1.5411E6	3.411E-3	0.4	1.9
26.996	300.0	2199.7	10000	20.0	5.368	117.996	175.0	600.0	0.2917	8544	8083.9600	0.02373	16168	1.6168E6	3.411E-3	0.4	2.0
27.996	300.0	2198.5	10000	20.0	5.372	118.996	175.0	600.1	0.2915	8550	8333.5498	0.02374	16667	1.6667E6	3.411E-3	0.5	2.0
28.996	300.0	2217.4	10000	20.0	5.374	119.996	176.5	600.0	0.2941	8553	8710.7002	0.02376	17421	1.7421E6	3.411E-3	0.5	2.0
29.996	300.0	2208.2	10000	20.0	5.366	120.996	175.7	600.0	0.2929	8541	8963.2100	0.02373	17926	1.7926E6	3.411E-3	0.5	2.0
30.996	300.0	2209.5	10000	20.0	5.366	121.996	175.8	600.1	0.2930	8541	9215.2695	0.02372	18431	1.8431E6	3.411E-3	0.5	2.0
31.996	300.0	2209.4	10000	20.0	5.380	122.996	175.8	600.0	0.2930	8562	9590.1797	0.02378	19180	1.9180E6	3.411E-3	0.5	2.0
32.996	300.0	2225.4	10000	20.0	5.371	123.996	177.1	600.0	0.2952	8549	9843.5596	0.02375	19687	1.9687E6	3.411E-3	0.5	2.1
33.996	300.0	2211.2	10000	20.0	5.379	124.996	176.0	600.0	0.2933	8561	10218.700	0.02378	20437	2.0437E6	3.411E-3	0.6	2.1
34.996	300.0	2222.3	10000	20.0	5.361	125.996	176.8	600.0	0.2948	8532	10471.700	0.02370	20943	2.0943E6	3.411E-3	0.6	2.1
35.996	300.0	2207.3	10000	20.0	5.368	126.996	175.7	600.0	0.2927	8543	10721.200	0.02373	21442	2.1442E6	3.411E-3	0.6	2.1
36.996	300.0	2223.4	10000	20.0	5.395	127.996	176.9	599.9	0.2949	8587	11098.300	0.02386	22197	2.2197E6	3.411E-3	0.6	2.1
37.996	300.0	2222.2	10000	20.0	5.387	128.996	176.8	600.0	0.2947	8573	11349.600	0.02382	22699	2.2699E6	3.411E-3	0.6	2.1
38.992	300.0	2213.1	10000	20.0	5.374	129.992	176.1	600.1	0.2935	8553	11600.800	0.02375	23202	2.3202E6	3.411E-3	0.6	2.2
39.992	300.0	2209.3	10000	20.0	5.363	130.992	175.8	600.0	0.2930	8535	11981.600	0.02371	23963	2.3963E6	3.411E-3	0.7	2.2
40.996	300.0	2202.6	10000	20.0	5.370	131.996	175.3	600.0	0.2921	8547	12230.100	0.02374	24460	2.4460E6	3.411E-3	0.7	2.2
41.996	300.0	2214.9	10000	20.0	5.388	132.996	176.3	600.0	0.2938	8576	12606.700	0.02382	25213	2.5213E6	3.411E-3	0.7	2.2
42.996	300.0	2216.2	10000	20.0	5.382	133.996	176.4	600.0	0.2939	8566	12859.900	0.02379	25720	2.5720E6	3.411E-3	0.7	2.2
43.996	300.0	2205.9	10000	20.0	5.365	134.996	175.5	600.0	0.2925	8538	13108.900	0.02372	26218	2.6218E6	3.411E-3	0.7	2.2
45.016	300.0	2204.6	10000	20.0	5.364	136.016	175.4	600.0	0.2924	8538	13486.000	0.02371	26972	2.6972E6	3.411E-3	0.8	2.3
45.996	300.0	2226.9	10000	20.0	5.367	136.996	177.2	600.0	0.2954	8542	13737.400	0.02373	27475	2.7475E6	3.411E-3	0.8	2.3
46.992	300.0	2209.9	10000	20.0	5.360	137.992	175.9	600.0	0.2931	8531	14114.400	0.02370	28229	2.8229E6	3.411E-3	0.8	2.3
48.000	300.0	2218.6	10000	20.0	5.380	139.000	176.5	600.0	0.2943	8562	14365.500	0.02379	28731	2.8731E6	3.411E-3	0.8	2.3
48.996	300.0	2237.0	10000	20.0	5.356	139.996	178.0	600.0	0.2967	8525	14617.000	0.02368	29234	2.9234E6	3.411E-3	0.8	2.3
50.000	300.0	2226.3	10000	20.0	5.375	141.000	177.2	600.0	0.2953	8554	14996.500	0.02376	29993	2.9993E6	3.411E-3	0.8	2.4
50.996	300.0	2196.8	10000	20.0	5.368	141.996	174.8	600.0	0.2913	8543	15245.200	0.02373	30490	3.0490E6	3.411E-3	0.8	2.4
51.996	300.0	2213.9	10000	20.0	5.357	142.996	176.2	600.0	0.2936	8526	15623.500	0.02368	31247	3.1247E6	3.411E-3	0.9	2.4
53.000	300.0	2216.4	10000	20.0	5.381	144.000	176.4	600.0	0.2940	8565	15875.100	0.02379	31750	3.1750E6	3.411E-3	0.9	2.4
53.996	300.0	2217.4	10000	20.0	5.366	144.996	176.5	600.0	0.2941	8540	16126.100	0.02372	32252	3.2252E6	3.411E-3	0.9	2.4
54.996	300.0	2207.9	10000	20.0	5.374	145.996	175.7	600.0	0.2928	8552	16501.699	0.02376	33003	3.3003E6	3.411E-3	0.9	2.4
55.996	300.0	2209.1	10000	20.0	5.380	146.996	175.8	600.0	0.2930	8563	16753.199	0.02379	33506	3.3506E6	3.411E-3	0.9	2.4
56.996	300.0	2231.6	10000	20.0	5.374	147.996	177.6	600.0	0.2960	8554	17004.400	0.02376	34009	3.4009E6	3.411E-3	0.9	2.5
57.996	300.0	2212.6	10000	20.0	5.368	148.996	176.1	600.0	0.2935	8543	17382.900	0.02373	34766	3.4766E6	3.411E-3	1.0	2.5
58.992	300.0	2205.1	10000	20.0	5.370	149.992	175.5	600.0	0.2925	8546	17633.801	0.02374	35268	3.5268E6	3.411E-3	1.0	2.5
59.996	300.0	2211.8	10000	20.0	5.360	150.996	176.0	600.0	0.2933	8530	18009.699	0.02369	36019	3.6019E6	3.411E-3	1.0	2.5

Continuous ramp step 2

time	velocity	torque	gap	temperature	normal force	time global	shear stress	shear rate	viscosity	normal stress	displacement	normal stress coefficient	strain	% strain	1/temperature	time	time global
s	rad/s	micro N.m	micro m	C	N	s	Pa	1/s	Pa.s	Pa	rad	Pa.s^2			1/K	min	min

1.0000	297.2	2175.3	10000	20.0	5.376	152.000	173.1	594.5	0.2912	8556	259.9500	0.02421	519.90	51990	3.411E-3	0.0	2.5
2.0160	291.2	2121.6	10000	20.0	5.384	153.016	168.8	582.4	0.2899	8569	616.8990	0.02526	1233.8	1.2338E5	3.411E-3	0.0	2.6
3.0040	287.1	2061.6	10000	20.0	5.398	154.004	164.1	574.3	0.2857	8590	854.9260	0.02605	1709.9	1.7099E5	3.411E-3	0.1	2.6
4.0160	283.0	2020.1	10000	20.0	5.421	155.016	160.8	565.9	0.2840	8628	1093.1100	0.02694	2186.2	2.1862E5	3.411E-3	0.1	2.6
5.0160	277.0	1958.4	10000	20.0	5.435	156.016	155.8	554.0	0.2813	8650	1431.1300	0.02819	2862.3	2.8623E5	3.411E-3	0.1	2.6
6.0000	272.9	1905.2	10000	20.0	5.435	157.000	151.6	545.8	0.2778	8650	1656.5200	0.02904	3313.0	3.3130E5	3.411E-3	0.1	2.6
7.0160	266.7	1839.0	10000	20.0	5.456	158.016	146.3	533.4	0.2744	8684	1994.7100	0.03052	3989.4	3.9894E5	3.411E-3	0.1	2.6
8.0160	262.7	1809.8	10000	20.0	5.468	159.016	144.0	525.3	0.2742	8703	2207.3601	0.03154	4414.7	4.4147E5	3.411E-3	0.1	2.7
9.0160	256.6	1727.7	10000	20.0	5.471	160.016	137.5	513.2	0.2679	8708	2526.7400	0.03307	5053.5	5.0535E5	3.411E-3	0.2	2.7
10.016	252.5	1674.3	10000	20.0	5.487	161.016	133.2	504.9	0.2639	8732	2739.5901	0.03425	5479.2	5.4792E5	3.411E-3	0.2	2.7
11.000	248.4	1652.4	10000	20.0	5.493	162.000	131.5	496.8	0.2647	8743	2939.8701	0.03543	5879.7	5.8797E5	3.411E-3	0.2	2.7
12.016	242.4	1593.5	10000	20.0	5.518	163.016	126.8	484.7	0.2616	8782	3240.3701	0.03738	6480.7	6.4807E5	3.411E-3	0.2	2.7
13.016	238.2	1549.5	10000	20.0	5.523	164.016	123.3	476.4	0.2588	8791	3442.0400	0.03873	6884.1	6.8841E5	3.411E-3	0.2	2.7
14.016	232.1	1478.3	10000	20.0	5.534	165.016	117.6	464.2	0.2534	8807	3728.5801	0.04087	7457.2	7.4572E5	3.411E-3	0.2	2.8
15.016	228.1	1446.8	10000	20.0	5.543	166.016	115.1	456.1	0.2524	8822	3916.1399	0.04240	7832.3	7.8323E5	3.411E-3	0.3	2.8
16.020	221.9	1381.1	10000	20.0	5.555	167.020	109.9	443.7	0.2477	8841	4199.4800	0.04490	8399.0	8.3990E5	3.411E-3	0.3	2.8
17.000	217.7	1331.6	10000	20.0	5.572	168.000	106.0	435.4	0.2434	8868	4379.1802	0.04677	8758.4	8.7584E5	3.411E-3	0.3	2.8
18.016	213.7	1316.0	10000	20.0	5.576	169.016	104.7	427.4	0.2450	8875	4555.1299	0.04859	9110.3	9.1103E5	3.411E-3	0.3	2.8
19.016	207.5	1236.7	10000	20.0	5.583	170.016	98.41	415.1	0.2371	8886	4816.9399	0.05157	9633.9	9.6339E5	3.411E-3	0.3	2.8
20.020	203.3	1204.1	10000	20.0	5.590	171.020	95.82	406.6	0.2357	8897	4993.2500	0.05382	9986.5	9.9865E5	3.411E-3	0.3	2.9
21.016	197.2	1155.4	10000	20.0	5.613	172.016	91.94	394.4	0.2331	8933	5236.0698	0.05744	10472	1.0472E6	3.411E-3	0.4	2.9
22.016	193.1	1110.2	10000	20.0	5.612	173.016	88.35	386.1	0.2288	8932	5402.2202	0.05991	10804	1.0804E6	3.411E-3	0.4	2.9
23.016	188.8	1074.0	10000	20.0	5.617	174.016	85.47	377.7	0.2263	8940	5561.1001	0.06267	11122	1.1122E6	3.411E-3	0.4	2.9
24.000	182.8	1015.9	10000	20.0	5.651	175.000	80.84	365.5	0.2212	8993	5785.9902	0.06731	11572	1.1572E6	3.411E-3	0.4	2.9
25.016	178.7	982.13	10000	20.0	5.645	176.016	78.16	357.3	0.2187	8984	5936.1201	0.07036	11872	1.1872E6	3.411E-3	0.4	2.9
26.020	172.3	929.34	10000	20.0	5.657	177.020	73.95	344.6	0.2146	9004	6161.6699	0.07582	12323	1.2323E6	3.411E-3	0.4	3.0
27.016	168.2	903.23	10000	20.0	5.670	178.016	71.88	336.4	0.2137	9024	6298.5000	0.07973	12597	1.2597E6	3.411E-3	0.5	3.0
28.016	164.1	857.93	10000	20.0	5.674	179.016	68.27	328.3	0.2080	9031	6436.6001	0.08381	12873	1.2873E6	3.411E-3	0.5	3.0
29.012	157.8	804.17	10000	20.0	5.677	180.012	63.99	315.6	0.2028	9035	6642.5898	0.09073	13285	1.3285E6	3.411E-3	0.5	3.0
30.016	153.7	771.89	10000	20.0	5.687	181.016	61.43	307.4	0.1998	9051	6770.0898	0.09575	13540	1.3540E6	3.411E-3	0.5	3.0
31.016	147.6	726.94	10000	20.0	5.700	182.016	57.85	295.1	0.1960	9072	6954.0898	0.1042	13908	1.3908E6	3.411E-3	0.5	3.0
32.016	143.3	695.66	10000	20.0	5.702	183.016	55.36	286.6	0.1932	9076	7079.5801	0.1105	14159	1.4159E6	3.411E-3	0.5	3.1
33.016	139.0	665.44	10000	20.0	5.709	184.016	52.95	278.1	0.1904	9086	7198.2402	0.1175	14396	1.4396E6	3.411E-3	0.6	3.1
34.016	132.9	609.10	10000	20.0	5.723	185.016	48.47	265.8	0.1823	9109	7365.9702	0.1289	14732	1.4732E6	3.411E-3	0.6	3.1
35.016	128.7	582.96	10000	20.0	5.727	186.016	46.39	257.3	0.1803	9115	7478.2202	0.1377	14956	1.4956E6	3.411E-3	0.6	3.1
36.016	124.4	559.22	10000	20.0	5.734	187.016	44.50	248.8	0.1789	9125	7584.1699	0.1474	15168	1.5168E6	3.411E-3	0.6	3.1
37.016	118.3	515.39	10000	20.0	5.744	188.016	41.01	236.6	0.1734	9142	7733.6899	0.1633	15467	1.5467E6	3.411E-3	0.6	3.1
38.016	114.0	485.06	10000	20.0	5.752	189.016	38.60	228.1	0.1692	9155	7833.3599	0.1760	15667	1.5667E6	3.411E-3	0.6	3.2
39.016	109.6	454.25	10000	20.0	5.766	190.016	36.15	219.3	0.1649	9177	7935.9502	0.1909	15872	1.5872E6	3.411E-3	0.7	3.2
40.016	103.4	415.55	10000	20.0	5.771	191.016	33.07	206.8	0.1599	9184	8064.3599	0.2147	16129	1.6129E6	3.411E-3	0.7	3.2
41.016	99.15	386.66	10000	20.0	5.765	192.016	30.77	198.3	0.1552	9175	8150.9199	0.2333	16302	1.6302E6	3.411E-3	0.7	3.2
42.000	94.70	360.52	10000	20.0	5.775	193.000	28.69	189.4	0.1515	9192	8237.9502	0.2562	16476	1.6476E6	3.411E-3	0.7	3.2
43.000	88.49	321.32	10000	20.0	5.784	194.000	25.57	177.0	0.1445	9206	8350.2305	0.2939	16700	1.6700E6	3.411E-3	0.7	3.2
44.016	84.21	303.77	10000	20.0	5.787	195.016	24.17	168.4	0.1435	9210	8424.2803	0.3247	16849	1.6849E6	3.411E-3	0.7	3.3
45.016	79.71	274.98	10000	20.0	5.792	196.016	21.88	159.4	0.1373	9218	8498.6602	0.3627	16997	1.6997E6	3.411E-3	0.8	3.3
46.016	73.50	239.04	10000	20.0	5.802	197.016	19.02	147.0	0.1294	9235	8591.8398	0.4274	17184	1.7184E6	3.411E-3	0.8	3.3
47.016	69.19	218.26	10000	20.0	5.801	198.016	17.37	138.4	0.1255	9233	8653.7598	0.4822	17308	1.7308E6	3.411E-3	0.8	3.3
48.000	64.62	199.03	10000	20.0	5.807	199.000	15.84	129.2	0.1226	9241	8715.5098	0.5533	17431	1.7431E6	3.411E-3	0.8	3.3
49.016	59.95	176.69	10000	20.0	5.811	200.016	14.06	119.9	0.1173	9248	8771.0400	0.6432	17542	1.7542E6	3.411E-3	0.8	3.3
50.012	55.72	154.15	10000	20.0	5.811	201.012	12.27	111.5	0.1101	9249	8820.5498	0.7446	17641	1.7641E6	3.411E-3	0.8	3.4
51.000	51.15	134.85	10000	20.0	5.817	202.000	10.73	102.3	0.1049	9259	8894.4805	0.8846	17789	1.7789E6	3.411E-3	0.9	3.4
52.000	43.79	106.96	10000	20.0	5.820	203.000	8.511	87.59	0.09717	9263	8937.2100	1.207	17874	1.7874E6	3.411E-3	0.9	3.4
53.016	39.42	88.519	10000	20.0	5.826	204.016	7.044	78.83	0.08936	9273	8973.9297	1.492	17948	1.7948E6	3.411E-3	0.9	3.4
54.016	34.51	72.470	10000	20.0	5.829	205.016	5.767	69.02	0.08356	9278	9010.3701	1.948	18021	1.8021E6	3.411E-3	0.9	3.4
55.016	29.36	56.546	10000	20.0	5.829	206.016	4.500	58.72	0.07664	9277	9040.6104	2.691	18081	1.8081E6	3.411E-3	0.9	3.4
56.016	24.93	43.564	10000	20.0	5.834	207.016	3.467	49.87	0.06952	9285	9064.7197	3.734	18129	1.8129E6	3.411E-3	0.9	3.5
57.000	19.63	29.536	10000	20.0	5.835	208.000	2.350	39.26	0.05986	9287	9088.4297	6.024	18177	1.8177E6	3.411E-3	1.0	3.5
58.016	16.43	22.487	10000	20.0	5.835	209.016	1.789	32.86	0.05446	9286	9099.7305	8.602	18199	1.8199E6	3.411E-3	1.0	3.5
59.000	11.33	11.990	10000	20.0	5.840	210.000	0.9541	22.65	0.04212	9295	9111.4404	18.11	18223	1.8223E6	3.411E-3	1.0	3.5
60.016	5.812	3.6074	10000	20.0	5.836	211.016	0.2871	11.62	0.02470	9288	9119.2900	68.74	18239	1.8239E6	3.411E-3	1.0	3.5

